SR103 - University of Central Florida
Principal Investigator: Yong-Ho Sohn
Project Title: Assessment of Failure Mechanisms for Thermal Barrier Coatings by
Photoluminescence, Electrochemical Impedance and Focused Ion Beam |
| Project Dates: |
May 2002 - October 2005 |
| Area of Research: |
Materials |
| Faculty-Student Inventory: |
Co-Principal Investigators: Vimal Desai and Lucille A. Giannuzzi
Ph.D.: Balaji Jarayaj
M.S.: Balaji Jarayaj, Barbara Franke, Srinivas Vishweswaraiah, Sankar Laxman
B.S.: Barbara Franke, Christopher Petorak, Travis Patterson,
D. Miranda
Research Assistants: Candice Wirth, Charles O'Toole, J. Liu,
J. Byeon, B. Jayaraj, , J.W. Byeon, A.M. Karlsson, B.W. Kempshall, S.K. Jha, R.R. Vanfleet, J. Kimmel, C.K. Lee, A.J. Burns,
R. Subramanian, B.W. Kempshall, L.A. Giannuzzi, K.S. Murphy |
| Collaborations: |
General Electric Aircraft Engines, Howmet International, Pratt & Whitney, Siemens-Westinghouse Power Corporation, and Solar Turbines Incorporated |
- Effects of Phase Constituents and Microstructure in Thermally Grown Oxide on The Thermal Cycling Lifetime and Failure of Thermal Barrier Coatings - Surface and Coatings Technology, Accepted for Publication, in Press, 2005
- Non-Destructive Evaluation of Degradation in Multi-Layered Thermal Barrier Coatings by Electrochemical Impedance Spectroscopy - Materials Science and Engineering A, Accepted for Publication, in Press, 2005
- Non-Destructive and Microstructural Characterization of Thermal Barrier Coatings - Journal of Metals, Vol. 56 (2004) 53-56
- An Observation of Nearly Failed Electron Beam Physical Vapor Deposited Thermal Barrier Coating with Grit Blasted (Ni,Pt)Al Bond Coat: Photostimulated Luminescence and Transmission Electron Microscopy - Thin Solid Films, Vol. 466 (2004) pp. 128-136
- Electrochemical Impedance Spectroscopy of Porous ZrO2 – 8 wt.% Y2O3 and Thermally Grown Oxide on Nickel Aluminide - Materials Science and Engineering A, Vol. A372 (2004) pp. 278-286
- Electrochemical Impedance Spectroscopy of Thermal Barrier Coatings as a Function of Isothermal and Cyclic Thermal Exposure - Surface and Coatings Technology, Vol. 177-178 (2004) pp. 140-151
- Microstructure of As-Coated Thermal Barrier Coatings with Varying Lifetimes - Surface and Coatings Technology, Vol. 177-178 (2004) pp. 89-96
- Phase Transformation of Thermally Grown Oxide on (Ni,Pt)Al Bond Coat During
Electron Beam Physical Vapor Deposition and Subsequent Oxidation - Surface and
Coatings Technology, Vol. 177-178 (2004) pp. 121-130
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UTSR PERFORMING MEMBER DIRECTORY
University of Central Florida |
Performing Member Contact:
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Vimal H. Desai, Associate Professor
University of Central Florida
Advanced Materials Processing and Analysis Center & Mechanical, Materials and Aerospace Engineering
Box 162455
Orlando , FL 32816-2450
407-882-1458/FAX 407-882-1462 vdesai@pegasus.cc.ucf.edu |
Experience |
- Combustion: Chemical kinetics, sensor development, ignition and exit profiles
- Heat Transfer/Aerodynamics: Film cooling, impingement cooling, rotating cooling channels, endwall/airfoil/tip heat transfer, conjugate heat transfer, computational fluid dynamics, supersonic flows, boundary element methods
- Materials: Thermal barrier coatings, oxidation, hot corrosion, steam oxidation, degradation of overlay protective coatings and superalloys, non-destructive evaluation, microstructural characterization
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Interest |
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Facilities |
- Combustion: Pressure-driven shock-tube with high-temperature and heterogeneous measurement capability; chemical kinetics modeling using Chemkin ; flame speeds measurement of realistic gas turbine mixtures at elevated pressure under development.
- Heat Transfer/Aerodynamics: Transonic, c losed loop transonic linear cascade facility for study of endwall, airfoil, and tip heat transfer, driv en by a 15,000 CFM fan with 100 inches of water pressure rise ; LN2-cooled, high density rat io film cooling with metal test coupons; flexible test rig for study of i mpingement cooling under a wide range o f test/geometric/flow conditions; computational fluid dynamics (CFD) facility with 36 node 3.06Ghz Intel Xeon Dell PowerEdge cluster with 108 GB RAM and 3.7 TB disc storage that benchmarks at 130 GFLOPS; 2D and 3D steady and transient boundary element codes for turbine applications; meshless methods codes for CFD and computational heat transfer.
- Materials: Isothermal and cyclic furnaces for oxidation and hot-corrosion, electrochemical impedance spectroscopy (EIS), photo-stimulated luminescence spectroscopy (PSLS), complete materials characterization facility including field-emission scanning electron microscope (FE-SEM), electron probe microanalysis (EPMA), focused ion beam (FIB) with ex-situ and in-situ lift-out (EXLO & INLO), transmission and scanning transmission electron microscope (TEM & STEM); thermal spray systems including plasma (APS) and high velocity oxy fuel (HVOF) systems under development.
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University of Central Florida
University of Central Florida , located in Orlando , Florida , celebrates its 40 th year with a current enrollment of over 40,000 students and research expenditure of nearly $100 million. UCF strives to become the “nation's leading metropolitan research university recognized for its intellectual, cultural, technological, and professional contributions and renowned for its outstanding programs and partnerships.” Research and education activities at UCF, related to turbine systems, including those supported by AGTSR and UTSR administered by SCIES, have made significantly contributions to technological development, student recruitment and, curriculum development. UCF has been awarded several times by AGTSR and UTSR in the area of combustion, heat transfer/aerodynamics and materials. These projects have also prompted other research grants from NSF, NASA and industrial partners.
Combustion: E. Petersen (petersen@mail.ucf.edu) Activity in the area of combustion includes fundamental measurements and analyses of chemical kinetics processes, including ignition, pyrolysis, and oxidation in gas-phase systems. Facilities include a pressure-driven shock-tube that provides the temperatures seen in gas turbine combustors in a controlled manner, yielding data for the calibration of chemical kinetics models and the development of empirical correlations. Chemical kinetics modeling is performed with the Chemkin suite of software. The capability for performing heterogeneous measurements such as spray combustion also exists with the UCF shock tube, and unique methods for performing such experiments are presently under development. Also under development is a facility for measuring the flame speeds of realistic gas turbine mixtures at elevated pressure.
Heat Transfer/Aerodynamics: J. Kapat (jkapat@mail.ucf.edu) and A. Kassab (kassab@mail.ucf.edu) Research in heat transfer and aerodynamics combine experimental and computational efforts on advanced cooling / heat transfer for endwall, airfoil, and tip. Experimental rig includes a transonic linear cascade for film cooling under representative Mach number. This rig can accommodate typical transition pieces at the inlet to the test section, and includes jet-grids for creation of high level of turbulence in a controlled fashion. Another rig provides LN2-cooled, high density ratio film cooling with metal test coupons, along with sophisticated dehumidification scheme for coolant injection with high density ratios. Computation research effort focuses on the fundamental development of boundary element methods in heat transfer and fluid dynamics with emphasis on conjugate heat transfer, coupled field problems, inverse problems, with applications in multidimensional heat transfer coefficient reconstruction, identification of contact resistance and thermal conductivity.
Materials: Y.H. Sohn (ysohn@mail.ucf.edu) and V.H. Desai (vdesai@mail.ucf.edu) Materials engineering for turbine applications have been one of the main thrust areas of research at UCF. Current and recent activities include assessment of failure mechanisms and non-destructive evaluation of thermal barrier coatings (TBCs), development of bond coats and overlay protective coatings, multicompoent-multiphase diffusion and phase transformation, steam oxidation of superalloys, repair technologies for superalloys, and environmental degradation of ceramic matrix composites (CMCs). Facility for materials engineering includes state-of-the-art characterization techniques, both non-destructive and microstructural, various thermal and environmental testing instruments, and processing techniques (under development) such as air plasma spray (APS) and high velocity oxy-fuel (HVOF) systems.
www.mmae.ucf.edu/~ysohn |
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