Services
Materials Characterization and Processing Center
A core component of our mission is to provide public service testing on a fee basis for Industry. Our center is committed to thoughtful problem-solving and analysis, a direct result of our in-depth technical experience and extensive knowledge gained, in part, via collaborations with faculty and industry partners. We are especially skilled at establishing non-routine, unique protocols to assist with a variety of needs, including troubleshooting, defect analysis, proof of concept, and pilot-scale testing and analysis.
Core Capabilities
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Chemical Analyses
- Determine chemical ‘makeup’ of materials
- Deconstruction of blends of materials by physical and chemical separation techniques
- FTIR spectroscopy
- Gas chromatography (GC) and GEL Permeation Chromatography (GPC)
- Accelerated Solvent Extractions (ASE)
- Optical microscopes (including hot stage microscope)
- Standard color viewing arrangements (lightboxes)
- Reflective color measurement systems for visual and numerical color characterization
- Absorbance of liquids in the visible range (to include ultra-violet and near-infrared absorbance/transmission properties of liquids/solutions using UV-Vis NIR spectroscopy)
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Non-Woven Research Services and Processes
- Production of non-woven materials such as air-laid processes, needle punching, hydroentanglement, sonic bonding and calendaring
- Carding and cross-lapping of fibers and non-woven materials
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ECE Clean Room Services and Processes
- Wet & dry chemical cleaning and etching
- Plasma etching
- ALD & E-beam deposited dielectrics & metals
- I-Line photolithography
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Thermal Analysis and Tensile Properties
- Determining key material properties such as:
- Degree of crystallinity
- Glass transition temperature
- Melting point range
- Degradation temperature
- Enthalpy of formation measurements via melt solution calorimetry
- Generate Stress/strain data
- Analyze data to determine tensile strength, elongation at break and tensile modules
- Instron testing with load cell capacities from 10 grams to 22,000 lbs
- Abrasion testing equipment
- Substrate porosity determination for all porous materials, including non-wovens and textiles
- Generate data such as mean pore size, pore size distribution, largest pore size and air the flux/permeability through materials being tested
- Determining key material properties such as:
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Modified Chemical Vapor Deposition Lathe
- Production of unique glass pre-form
- Recipe-based control of process variables
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Optical Fiber Draw Tower Services
- Wide range of temperatures and sizes
- Soft glass and polymer
- Particulate free and accurate specifications
Service Testing
As a department, we are able to offer the services of our Materials Characterization and Processing Center, which provides analytical and physical testing, manufacturing, fiber extrusion, and processing support and services. Please view our billing rates and equipment list for more details on commodities, services, and appropriate contacts.
---------Physical Testing
Jae Lowe
Phone: (864) 656-5972
Fax: (864) 656-5973
Email: Jaelowe@clemson.edu
Analytical Testing
Kim Ivey
(864) 656-5968
Fax: (864) 656-5973
Email: ikimber@clemson.edu
Department Equipment List
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Sample Preparation
Milli-Q Direct 8 Water purification system - Deionized water
Carver Laboratory Press Model B with 6" platens - Sample press, composites, sample preparation
Carver Laboratory Press Model C with 6" heated platens - Sample press, composites, sample preparation
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Balances
Sartorius Microbalance Model M2P - Mass determination, sample preparation
Mettler Toledo ME30 Microbalance - Mass determination, sample preparation
Sartorius Semi-Micro Analytical 6-place balance model LE 26D - Mass determination, sample preparation
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Extraction
Dionex ASE 300 Accelerated Solvent Extractor - Extraction, fiber finish quantification, sample preparation
Dionex ASE 200 Accelerated Solvent Extractor - Extraction, fiber finish quantification, sample preparation
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Thermal Analysis
TA Instruments Q400 TMA - Thermal mechanical analysis
TA Instruments Q5000 TGA - Thermo-gravimetric analysis
TA Instruments Q800 DMA - Dynamic Mechanical Analysis, Fiber/Film Tension Clamp, Dual/Single cantilever
TA Instruments TGA 2950 - Thermo-gravimetric analysis
TA Instruments MDSC 2920 - - Thermal Analysis, Differential Scanning Calorimetry, modulated DSC
TA Instruments Q1000 MDSC Thermal Analysis, Differential Scanning Calorimetry
Mettler Toledo DSC 823e - Thermal Analysis, Differential Scanning Calorimetry
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UV/VIS Spectroscopy
Shimadzu 3600 UV/Vis NIR - Ultraviolet, visible and near infrared spectroscopy
ISR-3100 UV/Vis NIR integrating sphere accessory for UV 3600 - Ultraviolet, visible and near infrared spectroscopy
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Infrared Spectroscopy
Thermo Nicolet Magna 550 FTIR - Fourier Transform Infrared Spectroscopy
Thermo-Spectra Tech Nic-Plan FTIR microscope - Fourier Transform Micro-Infrared Spectroscopy
Thermo-SpectraTech Foundation Series Diamond ATR Accessory - Attenuated Total Reflection Infrared Spectroscopy
Thermo 6700 FTIR Bench - Fourier Transform Infrared Spectroscopy
Thermo CONTINUUM FTIR Microscope - Fourier Transform Micro-Infrared Spectroscopy
Thermo- ORBIT ATR accessory with Diamond and Germanium plates - Attenuated Total Reflection Infrared Spectroscopy
Pike Technologies VEEMAX II Grazing Angle Accessory for FTIR - Grazing Angle Infrared spectroscopy
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Separations/Chromatography
Trace GC/MS (Thermo Finnigan) - Gas chromatography, mass spectroscopy
Waters GPC system with 1525 pump - Gel Permeation chromatography, polymer, Molecular weight distribution
Waters 2414 Refractive Index detector - Refractive Index, GPC detector
Waters 2477 UV/Vis detector - UV/Vis detection for GPC
Polymer Labs ELSD 2100 detector for GPC - Evaoporative light scattering
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Microscopy
Lawson-Hempill, Inc. DMT PPM-5R - Dynamic modulus tester
Instrument Color Systems multilight - LIGHTBOX - D65, A, CWF, UV lightbox
Pantone Color Viewing Lightbox - D65, cool white, flourescent lightbox
Meiji Techno RZ stereo microscope w/ ProgRes CapturePro software - Image analysis, stereomicroscopy
Jenoptik ProgRes SpeedXT core 5 CCD camera - CCD 5 megapixel high resolution camera
Techni-Quip Corp T-Q/FOI-1 Lamp - Sample illumination
Schott KL 1600 LED lamp - Sample illumination
Stocker and Yale, Inc. Lite Mite 9 Series Circular Illuminator, UV - Sample illumination
Circular Illuminator, blacklight - Sample illumination
Leitz Laborlux S compound microscope - Image analysis
Jenoptik ProgRes C5 CCD camera - 5 MP color CCD high resolution camera
CoolLED pE-100 illuminant for Leitz microscope - Sample illumination
Huvitz HRM-300 microscope with/ Panasis digital imaging software - High magnification imaging, 3D imaging and measurements, metallurgical
Lusis HC-20CU CCD camera - 2 MP color CCD high resolution camera
ausJena Jenapol Interphako interference microscope - Refractive index measurement
James Swift MP3502K microscope - Image analysis
Sony 3CCD camera - Color video camera
Mettler Toledo FP82HT Hotstage - Visual examination of thermal transitions in sample, microscopy
Mettler Toledo FP90 Central Processor - Hot stage control
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Physical Testing and Characterization
GretageMacbeth Color I 5 spectrophotometer - Color measurement, L*a*b* values, whiteness index
Buehler Ecomet 5 two-speed grinder-polisher - Sample grinding, polishing
Buehler Automet 2 powerhead - Ecomet 5 control
Instron Model 1125 with hydraulic, yarn, and fiber grips - Tensile strength testing, 10 N, 2000 g, 100 kg, and 1000 lb load cells
Instron Model 5582 - Tensile and compressive strength testing, 10 kN, 100 kN, 10 N load cells
Taber Abrader Model 503 - Abrasion testing, textiles
Wyzenbeek Abrader - Abrasion testing, textiles
Textest FX 3000 Hydrostatic Head Tester - Water resistance testing, hydrostatic head
Textest FX 3700 Elmendorf Tester - Tear strength testing
Textest FX 3300 Air Permeability Tester - Air permeability testing
PMI CFP-1000-AEXS Capillary Flow Tester - Pore size measurement
Mullen Tester - Burst strength measurement
Uster Tester 4 - Slub yarn analysis, mass variation, diagram, textile,
ILE DE-5 Digital Twist Counter - Twist count of single or plied yarn, textile
Sartorius MA50 Moisture Analyzer - Moisture content determination
Uster AFIS - Raw material analysis, nep, length, diameter, trash measurements, cotton
Lawson-Hemphill Constant Tension Transport - Spun yarn testing
Textechno Statimat M Automatic Tensile Tester - Tensile strength testing
Scott Tester Model J w/ Skein Tester - Skein tensile strength testing
Scott Tester Model J w/ ball burst tester - Ball burst tensile testing
USM Hytronic Cutting Machine Model B - Sample cutting, die cutting
Atlas Random Tumble Pilling Tester - Sample pilling measurement, textile
A.A.T.C.C. CM-5 Crockmeter - Color transference, scuffing, abrasion, flexing, powdering, dry-cleaning, textile
XRD Unit- Scintag Inc, Serial: 40074 - X-ray, crystallography
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Manufacturing
Ernst Benz Calendaring machine - Nonwoven bonding, point and area bonding, hot oil
Proctor and Schwartz Card - Cleaning, blending, direct card feed, open and randomize
Rando Feeder model 12 B - Fiber feeder for Rando Webber
Rando Webber model 12 C - Fiber web formation, air laid system, isotropic layered, width of 12"
Perfojet jet lace hydroentanglement system - Lightweight nonwoven production, hydroentanglement, 1000 psi
Ernst Benz TKF M500 oven, Aztec improved - Nonwoven textile heat setting, through-air oven
James Hunter Fiber Locker needling machine - Needle punching, 12" wide
James Hunter Pin-sonic Bonder - Ultrasonic bonding, vibrates at 20 kHz, 9" wide
Rando Prefeeder - Opening, blending
Rando Cleaner - Fiber cleaning for nonwoven line, feeds fiber into chute
Bematic Construzione Macchine Tessili - Carding, 20" wide
Impianti Automatex cross lapper conveyor - Layering lightweight web, 24" wide
Automatex Needle Loom - Bonding, 27" wide
Hills Inc Single Screw Extruder - Fiber extrusion
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Dyeing and Finishing
Despatch model LTC 2-12 oven - Textile drying, curing
Despatch model LTC 2-12 oven - Textile drying, curing
Speed Queen Drying Tumbler - Tumble drying
Erving Washer - Wash-fastness testing
Atlas Lauder-ometer model LHD-HT - Wash-fastness testing
Atlas Lauder-ometer model LHTP - Wash-fastness testing
Atlas Color Fade-ometer - Light-fastness testing
Ernst Benz Oven, Proctor and Schwartz Padder - Latex application on nonwoven, max width 15"
Milli-Pore Milli-Q Direct 8 water purification system - Deionized water
Roaches Colortec dyeing machine - Small package, beam, and loose fiber dyeing
Ahiba Texomat bench dye machine - Small sample dyeing
Werner Mathis AG DHE 39784 steamer oven - Universal steamer type
Sartorius CP16001 S Competence Analytical Balance - Large surface balance
4 ea Struers Labopol-5/Laboforce-3 polishing machine - Grinding, lapping, polishing
Struers Tegramin-20 - Polishing, specimen preparation, up to 4 specimens of 40mm dia
Buehler VibroMet 2 vibratory polisher - Polishing, 12" bowl size
Olympus BX60 Metallurgical microscope - Microscopy, imaging, image analysis, CCD 5 megapixel high resolution camera
Jenoptick ProgRes SpeedXT core 5 CCD camera and I-solutions software - Microscopy, imaging, image analysis, CCD 5 megapixel high resolution camera
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Furnaces
Lindberg Heavy Duti - Type: 59744 Serial: 10853
Lindberg Heavy Duti - Model: CC58125C Serial: UOSE-211167-UE
Lindberg - Type: 54233 Serial: 721024Lindberg Heavy Duti - Type: 54253 Serial: 7831
Lindberg - Type: 51442 Serial:879102
Thermodyne Over Series 9000 - Model: OV47335 Serial: 671990163682
Thermodyne Over Series 9000 - Model: OV47335 Serial: 671930574328
Lindberg - Type: 51333 Serial:12878
Lindberg - Model: STF54453C Serial: TIIL-533879-TL
Applied Test Systems, Inc - Serial: 9361A
Lindberg - Type: 54032-A Serial:114644
Lindberg - Type: 54314 Serial: 909199
Lindberg - Type: 51314 Serial: 848026
KH Huppert Co - Serial: 101 Type: SP
Thermcraft Inc - Model: FCR-10-0-10-1C-J53007/6A Serial: 005307/6A</p
Thermcraft Inc - Model: FCR-10-0-10-1C-J53007/6B Serial: 005307/6B
Thermcraft Inc - Model: FCR-10-0-10-1C-J53007/6C Serial: 005307/6C
Lindberg Blue - Type: HTF55347C Serial: T12L-534116-TL
Lindberg Blue - Type: STF-54453C Serial: T11L-533880-TL Tube Furnace
Lindberg - Type: 51333 Serial: 899116
Lindberg - Model: S51644 Serial:919162
Deltech Inc
Lindberg
Grieve
Lindberg Blue
Pereco - Model: 2600-112
Thermcraft Inc - Model: FBM-24-24-30-1F-J5307/1A Serial: 005307/1A
Grieve - Model: AA-1250 Serial: 340093