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Materials Science and Engineering

Services

Materials Characterization and Processing Center

A core component of our mission is to provide public service testing on a fee basis for Industry. Our center is committed to thoughtful problem-solving and analysis, a direct result of our in-depth technical experience and extensive knowledge gained, in part, via collaborations with faculty and industry partners. We are especially skilled at establishing non-routine, unique protocols to assist with a variety of needs, including troubleshooting, defect analysis, proof of concept, and pilot-scale testing and analysis.

Core Capabilities

  • Chemical Analyses
    • Determine chemical ‘makeup’ of materials
    • Deconstruction of blends of materials by physical and chemical separation techniques
    • FTIR spectroscopy
    • Gas chromatography (GC) and GEL Permeation Chromatography (GPC)
    • Accelerated Solvent Extractions (ASE)
    • Optical microscopes (including hot stage microscope)
    • Standard color viewing arrangements (lightboxes)
    • Reflective color measurement systems for visual and numerical color characterization
    • Absorbance of liquids in the visible range (to include ultra-violet and near-infrared absorbance/transmission properties of liquids/solutions using UV-Vis NIR spectroscopy)
  • Non-Woven Research Services and Processes
    • Production of non-woven materials such as air-laid processes, needle punching, hydroentanglement, sonic bonding and calendaring
    • Carding and cross-lapping of fibers and non-woven materials
  • ECE Clean Room Services and Processes
    • Wet & dry chemical cleaning and etching
    • Plasma etching
    • ALD & E-beam deposited dielectrics & metals
    • I-Line photolithography
  • Thermal Analysis and Tensile Properties
    • Determining key material properties such as:
      • Degree of crystallinity
      • Glass transition temperature
      • Melting point range
      • Degradation temperature
      • Enthalpy of formation measurements via melt solution calorimetry
    • Generate Stress/strain data
    • Analyze data to determine tensile strength, elongation at break and tensile modules
    • Instron testing with load cell capacities from 10 grams to 22,000 lbs
    • Abrasion testing equipment
    • Substrate porosity determination for all porous materials, including non-wovens and textiles
    • Generate data such as mean pore size, pore size distribution, largest pore size and air the flux/permeability through materials being tested
  • Modified Chemical Vapor Deposition Lathe
    • Production of unique glass pre-form
    • Recipe-based control of process variables
  • Optical Fiber Draw Tower Services
    • Wide range of temperatures and sizes
    • Soft glass and polymer
    • Particulate free and accurate specifications

Service Testing

As a department, we are able to offer the services of our Materials Characterization and Processing Center, which provides analytical and physical testing, manufacturing, fiber extrusion, and processing support and services. Please view our billing rates and equipment list for more details on commodities, services, and appropriate contacts.

Billing Rates
Equipment List

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Physical Testing
Jae Lowe
Phone: (864) 656-5972
Fax: (864) 656-5973
Email: Jaelowe@clemson.edu

Analytical Testing
Kim Ivey
(864) 656-5968
Fax: (864) 656-5973
Email: ikimber@clemson.edu

Department Equipment List

  • Sample Preparation

    Milli-Q Direct 8 Water purification system - Deionized water

    Carver Laboratory Press Model B with 6" platens - Sample press, composites, sample preparation

    Carver Laboratory Press Model C with 6" heated platens - Sample press, composites, sample preparation

  • Balances

    Sartorius Microbalance Model M2P - Mass determination, sample preparation

    Mettler Toledo ME30 Microbalance - Mass determination, sample preparation

    Sartorius Semi-Micro Analytical 6-place balance model LE 26D - Mass determination, sample preparation

  • Extraction

    Dionex ASE 300 Accelerated Solvent Extractor - Extraction, fiber finish quantification, sample preparation

    Dionex ASE 200 Accelerated Solvent Extractor - Extraction, fiber finish quantification, sample preparation

  • Thermal Analysis

    TA Instruments Q400 TMA - Thermal mechanical analysis

    TA Instruments Q5000 TGA - Thermo-gravimetric analysis

    TA Instruments Q800 DMA - Dynamic Mechanical Analysis, Fiber/Film Tension Clamp, Dual/Single cantilever

    TA Instruments TGA 2950 - Thermo-gravimetric analysis

    TA Instruments MDSC 2920 - - Thermal Analysis, Differential Scanning Calorimetry, modulated DSC

    TA Instruments Q1000 MDSC Thermal Analysis, Differential Scanning Calorimetry

    Mettler Toledo DSC 823e - Thermal Analysis, Differential Scanning Calorimetry

  • UV/VIS Spectroscopy

    Shimadzu 3600 UV/Vis NIR - Ultraviolet, visible and near infrared spectroscopy

    ISR-3100 UV/Vis NIR integrating sphere accessory for UV 3600 - Ultraviolet, visible and near infrared spectroscopy

  • Infrared Spectroscopy

    Thermo Nicolet Magna 550 FTIR - Fourier Transform Infrared Spectroscopy

    Thermo-Spectra Tech Nic-Plan FTIR microscope - Fourier Transform Micro-Infrared Spectroscopy

    Thermo-SpectraTech Foundation Series Diamond ATR Accessory - Attenuated Total Reflection Infrared Spectroscopy

    Thermo 6700 FTIR Bench - Fourier Transform Infrared Spectroscopy

    Thermo CONTINUUM FTIR Microscope - Fourier Transform Micro-Infrared Spectroscopy

    Thermo- ORBIT ATR accessory with Diamond and Germanium plates - Attenuated Total Reflection Infrared Spectroscopy

    Pike Technologies VEEMAX II Grazing Angle Accessory for FTIR - Grazing Angle Infrared spectroscopy

  • Separations/Chromatography

    Trace GC/MS (Thermo Finnigan) - Gas chromatography, mass spectroscopy

    Waters GPC system with 1525 pump - Gel Permeation chromatography, polymer, Molecular weight distribution

    Waters 2414 Refractive Index detector - Refractive Index, GPC detector

    Waters 2477 UV/Vis detector - UV/Vis detection for GPC

    Polymer Labs ELSD 2100 detector for GPC - Evaoporative light scattering

  • Microscopy

    Lawson-Hempill, Inc. DMT PPM-5R - Dynamic modulus tester

    Instrument Color Systems multilight - LIGHTBOX - D65, A, CWF, UV lightbox

    Pantone Color Viewing Lightbox - D65, cool white, flourescent lightbox

    Meiji Techno RZ stereo microscope w/ ProgRes CapturePro software - Image analysis, stereomicroscopy

    Jenoptik ProgRes SpeedXT core 5 CCD camera - CCD 5 megapixel high resolution camera

    Techni-Quip Corp T-Q/FOI-1 Lamp - Sample illumination

    Schott KL 1600 LED lamp - Sample illumination

    Stocker and Yale, Inc. Lite Mite 9 Series Circular Illuminator, UV - Sample illumination

    Circular Illuminator, blacklight - Sample illumination

    Leitz Laborlux S compound microscope - Image analysis

    Jenoptik ProgRes C5 CCD camera - 5 MP color CCD high resolution camera

    CoolLED pE-100 illuminant for Leitz microscope - Sample illumination

    Huvitz HRM-300 microscope with/ Panasis digital imaging software - High magnification imaging, 3D imaging and measurements, metallurgical

    Lusis HC-20CU CCD camera - 2 MP color CCD high resolution camera

    ausJena Jenapol Interphako interference microscope - Refractive index measurement

    James Swift MP3502K microscope - Image analysis

    Sony 3CCD camera - Color video camera

    Mettler Toledo FP82HT Hotstage - Visual examination of thermal transitions in sample, microscopy

    Mettler Toledo FP90 Central Processor - Hot stage control

  • Physical Testing and Characterization

    GretageMacbeth Color I 5 spectrophotometer - Color measurement, L*a*b* values, whiteness index

    Buehler Ecomet 5 two-speed grinder-polisher - Sample grinding, polishing

    Buehler Automet 2 powerhead - Ecomet 5 control

    Instron Model 1125 with hydraulic, yarn, and fiber grips - Tensile strength testing, 10 N, 2000 g, 100 kg, and 1000 lb load cells

    Instron Model 5582 - Tensile and compressive strength testing, 10 kN, 100 kN, 10 N load cells

    Taber Abrader Model 503 - Abrasion testing, textiles

    Wyzenbeek Abrader - Abrasion testing, textiles

    Textest FX 3000 Hydrostatic Head Tester - Water resistance testing, hydrostatic head

    Textest FX 3700 Elmendorf Tester - Tear strength testing

    Textest FX 3300 Air Permeability Tester - Air permeability testing

    PMI CFP-1000-AEXS Capillary Flow Tester - Pore size measurement

    Mullen Tester - Burst strength measurement

    Uster Tester 4 - Slub yarn analysis, mass variation, diagram, textile,

    ILE DE-5 Digital Twist Counter - Twist count of single or plied yarn, textile

    Sartorius MA50 Moisture Analyzer - Moisture content determination

    Uster AFIS - Raw material analysis, nep, length, diameter, trash measurements, cotton

    Lawson-Hemphill Constant Tension Transport - Spun yarn testing

    Textechno Statimat M Automatic Tensile Tester - Tensile strength testing

    Scott Tester Model J w/ Skein Tester - Skein tensile strength testing

    Scott Tester Model J w/ ball burst tester - Ball burst tensile testing

    USM Hytronic Cutting Machine Model B - Sample cutting, die cutting

    Atlas Random Tumble Pilling Tester - Sample pilling measurement, textile

    A.A.T.C.C. CM-5 Crockmeter - Color transference, scuffing, abrasion, flexing, powdering, dry-cleaning, textile

    XRD Unit- Scintag Inc, Serial: 40074 - X-ray, crystallography

  • Manufacturing

    Ernst Benz Calendaring machine - Nonwoven bonding, point and area bonding, hot oil

    Proctor and Schwartz Card - Cleaning, blending, direct card feed, open and randomize

    Rando Feeder model 12 B - Fiber feeder for Rando Webber

    Rando Webber model 12 C - Fiber web formation, air laid system, isotropic layered, width of 12"

    Perfojet jet lace hydroentanglement system - Lightweight nonwoven production, hydroentanglement, 1000 psi

    Ernst Benz TKF M500 oven, Aztec improved - Nonwoven textile heat setting, through-air oven

    James Hunter Fiber Locker needling machine - Needle punching, 12" wide

    James Hunter Pin-sonic Bonder - Ultrasonic bonding, vibrates at 20 kHz, 9" wide

    Rando Prefeeder - Opening, blending

    Rando Cleaner - Fiber cleaning for nonwoven line, feeds fiber into chute

    Bematic Construzione Macchine Tessili - Carding, 20" wide

    Impianti Automatex cross lapper conveyor - Layering lightweight web, 24" wide

    Automatex Needle Loom - Bonding, 27" wide

    Hills Inc Single Screw Extruder - Fiber extrusion

  • Dyeing and Finishing

    Despatch model LTC 2-12 oven - Textile drying, curing

    Despatch model LTC 2-12 oven - Textile drying, curing

    Speed Queen Drying Tumbler - Tumble drying

    Erving Washer - Wash-fastness testing

    Atlas Lauder-ometer model LHD-HT - Wash-fastness testing

    Atlas Lauder-ometer model LHTP - Wash-fastness testing

    Atlas Color Fade-ometer - Light-fastness testing

    Ernst Benz Oven, Proctor and Schwartz Padder - Latex application on nonwoven, max width 15"

    Milli-Pore Milli-Q Direct 8 water purification system - Deionized water

    Roaches Colortec dyeing machine - Small package, beam, and loose fiber dyeing

    Ahiba Texomat bench dye machine - Small sample dyeing

    Werner Mathis AG DHE 39784 steamer oven - Universal steamer type

    Sartorius CP16001 S Competence Analytical Balance - Large surface balance

    4 ea Struers Labopol-5/Laboforce-3 polishing machine - Grinding, lapping, polishing

    Struers Tegramin-20 - Polishing, specimen preparation, up to 4 specimens of 40mm dia

    Buehler VibroMet 2 vibratory polisher - Polishing, 12" bowl size

    Olympus BX60 Metallurgical microscope - Microscopy, imaging, image analysis, CCD 5 megapixel high resolution camera

    Jenoptick ProgRes SpeedXT core 5 CCD camera and I-solutions software - Microscopy, imaging, image analysis, CCD 5 megapixel high resolution camera

  • Furnaces

    Lindberg Heavy Duti - Type: 59744 Serial: 10853

    Lindberg Heavy Duti - Model: CC58125C Serial: UOSE-211167-UE

    Lindberg - Type: 54233 Serial: 721024Lindberg Heavy Duti - Type: 54253 Serial: 7831

    Lindberg - Type: 51442 Serial:879102

    Thermodyne Over Series 9000 - Model: OV47335 Serial: 671990163682

    Thermodyne Over Series 9000 - Model: OV47335 Serial: 671930574328

    Lindberg - Type: 51333 Serial:12878

    Lindberg - Model: STF54453C Serial: TIIL-533879-TL

    Applied Test Systems, Inc - Serial: 9361A

    Lindberg - Type: 54032-A Serial:114644

    Lindberg - Type: 54314 Serial: 909199

    Lindberg - Type: 51314 Serial: 848026

    KH Huppert Co - Serial: 101 Type: SP

    Thermcraft Inc - Model: FCR-10-0-10-1C-J53007/6A Serial: 005307/6A</p

    Thermcraft Inc - Model: FCR-10-0-10-1C-J53007/6B Serial: 005307/6B

    Thermcraft Inc - Model: FCR-10-0-10-1C-J53007/6C Serial: 005307/6C

    Lindberg Blue - Type: HTF55347C Serial: T12L-534116-TL

    Lindberg Blue - Type: STF-54453C Serial: T11L-533880-TL Tube Furnace

    Lindberg - Type: 51333 Serial: 899116

    Lindberg - Model: S51644 Serial:919162

    Deltech Inc

    Lindberg

    Grieve

    Lindberg Blue

    Pereco - Model: 2600-112

    Thermcraft Inc - Model: FBM-24-24-30-1F-J5307/1A Serial: 005307/1A

    Grieve - Model: AA-1250 Serial: 340093